Specifications
-
CRM State:
-
Matrix:
-
Mineralisation:
OREAS 349 is a replacement for OREAS 350. It is a zinc concentrate certified reference material (CRM) sourced from the McArthur River Mining operation located in the Gulf of Carpentaria region in the Northern Territory of Australia. The mine is situated about 900 km southeast of Darwin. The major sulphides are pyrite, sphalerite and galena, with lesser chalcopyrite, arsenopyrite and marcasite. Twenty-eight laboratories participated in the certification program to determine:
Analyte | Certified Value | 1SD | Expanded Uncertainty Low | Expanded Uncertainty High | Method |
---|---|---|---|---|---|
Zn, Zinc (wt.%) | 43.49 | 0.185 | 43.38 | 43.60 | Classical Wet Chemistry |
Zn, Zinc (wt.%) | 44.03 | 1.067 | 42.64 | 45.43 | 4-Acid Digestion |
Pb, Lead (wt.%) | 2.19 | 0.062 | 2.13 | 2.25 | 4-Acid Digestion |
Ag, Silver (ppm) | 85.8 | 1.77 | 83.4 | 88.2 | 4-Acid Digestion |
Al, Aluminium (wt.%) | 0.816 | 0.037 | 0.791 | 0.841 | 4-Acid Digestion |
As, Arsenic (ppm) | 565 | 17 | 542 | 587 | 4-Acid Digestion |
Be, Beryllium (ppm) | < 0.50 | IND | IND | IND | 4-Acid Digestion |
Bi, Bismuth (ppm) | 61 | 3.8 | 57 | 65 | 4-Acid Digestion |
Ca, Calcium (wt.%) | 0.621 | 0.020 | 0.602 | 0.639 | 4-Acid Digestion |
Cd, Cadmium (wt.%) | 0.116 | 0.004 | 0.113 | 0.119 | 4-Acid Digestion |
Ce, Cerium (ppm) | 10.4 | 1.3 | 9.1 | 11.7 | 4-Acid Digestion |
Co, Cobalt (ppm) | 127 | 9 | 121 | 133 | 4-Acid Digestion |
Cr, Chromium (ppm) | 99 | 13 | 88 | 110 | 4-Acid Digestion |
Cs, Caesium (ppm) | 0.59 | 0.036 | 0.53 | 0.65 | 4-Acid Digestion |
Cu, Copper (wt.%) | 1.42 | 0.031 | 1.38 | 1.45 | 4-Acid Digestion |
Dy, Dysprosium (ppm) | 0.60 | 0.08 | 0.42 | 0.78 | 4-Acid Digestion |
Er, Erbium (ppm) | 0.38 | 0.04 | 0.27 | 0.49 | 4-Acid Digestion |
Eu, Europium (ppm) | 0.29 | 0.05 | 0.18 | 0.40 | 4-Acid Digestion |
Fe, Iron (wt.%) | 9.23 | 0.306 | 8.99 | 9.46 | 4-Acid Digestion |
Ga, Gallium (ppm) | 11.6 | 0.67 | 10.8 | 12.4 | 4-Acid Digestion |
Gd, Gadolinium (ppm) | 0.82 | 0.072 | 0.66 | 0.97 | 4-Acid Digestion |
Hf, Hafnium (ppm) | 0.64 | 0.07 | 0.52 | 0.75 | 4-Acid Digestion |
In, Indium (ppm) | 35.4 | 2.05 | 33.4 | 37.4 | 4-Acid Digestion |
K, Potassium (wt.%) | 0.226 | 0.006 | 0.216 | 0.236 | 4-Acid Digestion |
Li, Lithium (ppm) | 3.03 | 0.31 | 2.66 | 3.40 | 4-Acid Digestion |
Mg, Magnesium (wt.%) | 0.265 | 0.014 | 0.253 | 0.276 | 4-Acid Digestion |
Mn, Manganese (wt.%) | 0.464 | 0.008 | 0.453 | 0.475 | 4-Acid Digestion |
Mo, Molybdenum (ppm) | 170 | 7 | 164 | 177 | 4-Acid Digestion |
Na, Sodium (wt.%) | 0.173 | 0.007 | 0.165 | 0.181 | 4-Acid Digestion |
Nb, Niobium (ppm) | 0.90 | 0.09 | 0.80 | 1.01 | 4-Acid Digestion |
Nd, Neodymium (ppm) | 4.88 | 0.305 | 4.30 | 5.47 | 4-Acid Digestion |
Ni, Nickel (ppm) | 74 | 4.0 | 71 | 78 | 4-Acid Digestion |
P, Phosphorus (wt.%) | 0.011 | 0.001 | 0.010 | 0.012 | 4-Acid Digestion |
Pr, Praseodymium (ppm) | 1.27 | 0.118 | 1.10 | 1.45 | 4-Acid Digestion |
Rb, Rubidium (ppm) | 9.55 | 0.323 | 8.90 | 10.19 | 4-Acid Digestion |
Re, Rhenium (ppm) | 0.11 | 0.01 | 0.09 | 0.13 | 4-Acid Digestion |
S, Sulphur (wt.%) | 28.56 | 1.378 | 27.49 | 29.63 | 4-Acid Digestion |
Sb, Antimony (ppm) | 689 | 45 | 658 | 720 | 4-Acid Digestion |
Sc, Scandium (ppm) | 1.54 | 0.124 | 1.37 | 1.71 | 4-Acid Digestion |
Se, Selenium (ppm) | 27.1 | 4.0 | 23.4 | 30.8 | 4-Acid Digestion |
Sm, Samarium (ppm) | 0.98 | 0.080 | 0.79 | 1.16 | 4-Acid Digestion |
Sn, Tin (ppm) | 11.3 | 1.10 | 10.1 | 12.6 | 4-Acid Digestion |
Sr, Strontium (ppm) | 41.2 | 5.9 | 36.9 | 45.4 | 4-Acid Digestion |
Ta, Tantalum (ppm) | 0.082 | 0.013 | 0.064 | 0.099 | 4-Acid Digestion |
Te, Tellurium (ppm) | 1.79 | 0.22 | 1.56 | 2.01 | 4-Acid Digestion |
Th, Thorium (ppm) | 1.55 | 0.29 | 1.27 | 1.84 | 4-Acid Digestion |
Ti, Titanium (wt.%) | 0.040 | 0.003 | 0.038 | 0.043 | 4-Acid Digestion |
Tl, Thallium (ppm) | 20.0 | 1.78 | 18.4 | 21.6 | 4-Acid Digestion |
U, Uranium (ppm) | 1.59 | 0.073 | 1.48 | 1.70 | 4-Acid Digestion |
V, Vanadium (ppm) | 13.2 | 1.6 | 11.7 | 14.6 | 4-Acid Digestion |
W, Tungsten (ppm) | 4.19 | 0.268 | 3.84 | 4.54 | 4-Acid Digestion |
Y, Yttrium (ppm) | 3.55 | 0.202 | 3.25 | 3.84 | 4-Acid Digestion |
Yb, Ytterbium (ppm) | 0.35 | 0.04 | 0.24 | 0.47 | 4-Acid Digestion |
Zr, Zirconium (ppm) | 22.8 | 1.06 | 21.6 | 24.0 | 4-Acid Digestion |
S, Sulphur (wt.%) | 30.22 | 0.897 | 29.53 | 30.91 | Infrared Combustion |
Al, Aluminium (wt.%) | 0.847 | 0.020 | 0.823 | 0.871 | Peroxide Fusion ICP |
As, Arsenic (ppm) | 606 | 35 | 577 | 634 | Peroxide Fusion ICP |
Ba, Barium (ppm) | 816 | 37 | 775 | 857 | Peroxide Fusion ICP |
Be, Beryllium (ppm) | < 1.00 | IND | IND | IND | Peroxide Fusion ICP |
Bi, Bismuth (ppm) | 62 | 3.3 | 57 | 66 | Peroxide Fusion ICP |
Ca, Calcium (wt.%) | 0.648 | 0.058 | 0.593 | 0.704 | Peroxide Fusion ICP |
Cd, Cadmium (wt.%) | 0.116 | 0.007 | 0.108 | 0.123 | Peroxide Fusion ICP |
Ce, Cerium (ppm) | 11.3 | 0.91 | 10.1 | 12.5 | Peroxide Fusion ICP |
Co, Cobalt (ppm) | 127 | 10 | 118 | 136 | Peroxide Fusion ICP |
Cr, Chromium (ppm) | 116 | 31 | 91 | 141 | Peroxide Fusion ICP |
Cu, Copper (wt.%) | 1.43 | 0.019 | 1.40 | 1.46 | Peroxide Fusion ICP |
Fe, Iron (wt.%) | 9.42 | 0.175 | 9.20 | 9.64 | Peroxide Fusion ICP |
Ga, Gallium (ppm) | 12.2 | 1.4 | 10.2 | 14.3 | Peroxide Fusion ICP |
Gd, Gadolinium (ppm) | 0.95 | 0.11 | 0.71 | 1.18 | Peroxide Fusion ICP |
In, Indium (ppm) | 36.0 | 2.32 | 32.6 | 39.3 | Peroxide Fusion ICP |
K, Potassium (wt.%) | 0.251 | 0.043 | 0.220 | 0.283 | Peroxide Fusion ICP |
La, Lanthanum (ppm) | 6.57 | 0.473 | 5.86 | 7.28 | Peroxide Fusion ICP |
Mg, Magnesium (wt.%) | 0.280 | 0.012 | 0.269 | 0.290 | Peroxide Fusion ICP |
Mn, Manganese (wt.%) | 0.472 | 0.014 | 0.457 | 0.487 | Peroxide Fusion ICP |
Mo, Molybdenum (ppm) | 176 | 15 | 162 | 190 | Peroxide Fusion ICP |
Nd, Neodymium (ppm) | 5.14 | 0.392 | 4.51 | 5.76 | Peroxide Fusion ICP |
Ni, Nickel (ppm) | 79 | 12 | 64 | 93 | Peroxide Fusion ICP |
Pb, Lead (wt.%) | 2.18 | 0.055 | 2.13 | 2.24 | Peroxide Fusion ICP |
Pr, Praseodymium (ppm) | 1.35 | 0.081 | 1.18 | 1.52 | Peroxide Fusion ICP |
Rb, Rubidium (ppm) | 10.2 | 0.67 | 9.0 | 11.3 | Peroxide Fusion ICP |
S, Sulphur (wt.%) | 29.97 | 0.769 | 29.22 | 30.73 | Peroxide Fusion ICP |
Sb, Antimony (ppm) | 731 | 46 | 684 | 779 | Peroxide Fusion ICP |
Si, Silicon (wt.%) | 2.96 | 0.087 | 2.86 | 3.06 | Peroxide Fusion ICP |
Sm, Samarium (ppm) | 1.01 | 0.075 | 0.83 | 1.20 | Peroxide Fusion ICP |
Sr, Strontium (ppm) | 50 | 3.9 | 46 | 54 | Peroxide Fusion ICP |
Th, Thorium (ppm) | 1.93 | 0.171 | 1.71 | 2.15 | Peroxide Fusion ICP |
Ti, Titanium (wt.%) | 0.046 | 0.004 | 0.041 | 0.050 | Peroxide Fusion ICP |
Tl, Thallium (ppm) | 20.7 | 0.98 | 19.3 | 22.1 | Peroxide Fusion ICP |
Tm, Thulium (ppm) | < 0.10 | IND | IND | IND | Peroxide Fusion ICP |
U, Uranium (ppm) | 1.74 | 0.155 | 1.55 | 1.93 | Peroxide Fusion ICP |
V, Vanadium (ppm) | 18.0 | 3.1 | 14.7 | 21.2 | Peroxide Fusion ICP |
W, Tungsten (ppm) | 4.94 | 0.62 | 3.77 | 6.11 | Peroxide Fusion ICP |
Y, Yttrium (ppm) | 4.44 | 0.414 | 3.91 | 4.98 | Peroxide Fusion ICP |
Yb, Ytterbium (ppm) | 0.44 | 0.08 | 0.23 | 0.64 | Peroxide Fusion ICP |
Zn, Zinc (wt.%) | 43.96 | 0.725 | 43.10 | 44.83 | Peroxide Fusion ICP |